2-Bromo-6-(trifluoromethoxy)quinoline

Base Information

Chemical Name:2-Bromo-6-(trifluoromethoxy)quinoline
CAS No.:1352443-11-8
Molecular Formula:C₁₀H₅BrF₃NO
Molecular Weight:292.055
Hs Code.:

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Chemical Property of 2-Bromo-6-(trifluoromethoxy)quinoline

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Technology Process of 2-Bromo-6-(trifluoromethoxy)quinoline

There total 3 articles about 2-Bromo-6-(trifluoromethoxy)quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.7%

: 676131-26-3
6-trifluoromethoxyquinoline-1-oxide

: 1352443-11-8
2-Bromo-6-(trifluoromethoxy)quinoline

Guidance literature:: 6-trifluoromethoxyquinoline-1-oxide; With acetic anhydride; at 130 - 140 ℃; for 5h; Inert atmosphere;

With phosphorus(V) oxybromide; at 130 - 140 ℃; for 4h; Inert atmosphere;

Reference yield:

: 461-82-5
4-(trifluoromethoxy)aniline

: 1352443-11-8
2-Bromo-6-(trifluoromethoxy)quinoline

Guidance literature:: Multi-step reaction with 3 steps

1.1: boric acid; ferrous(II) sulfate heptahydrate; sulfuric acid / water; glycerol / 0 - 150 °C

2.1: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 0 - 20 °C

3.1: acetic anhydride / 5 h / 130 - 140 °C / Inert atmosphere

3.2: 4 h / 130 - 140 °C / Inert atmosphere

With ferrous(II) sulfate heptahydrate; sulfuric acid; boric acid; acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In water; ethyl acetate; glycerol;

Reference yield:

: 212695-45-9
6-(trifluoromethoxy)quinoline

: 1352443-11-8
2-Bromo-6-(trifluoromethoxy)quinoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 0 - 20 °C

2.1: acetic anhydride / 5 h / 130 - 140 °C / Inert atmosphere

2.2: 4 h / 130 - 140 °C / Inert atmosphere

With acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In ethyl acetate;