(R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester

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Chemical Name:(R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester
CAS No.:87357-75-3
Molecular Formula:C₆₈H₁₀₂N₂O₁₅
Molecular Weight:1187.56
Hs Code.:

(R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester

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Chemical Property of (R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester

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Technology Process of (R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester

There total 9 articles about (R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88862-41-3
C₇₁H₁₀₆N₂O₁₅

: 87357-75-3
(R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: With acetic acid; at 90 ℃; for 0.333333h; Yield given;
DOI:10.1016/S0040-4039(00)81830-4

Reference yield:

: 28715-21-1,3422-31-9
(R)-3-hydroxytetradecanoic acid

: 87357-75-3
(R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / Et₃N / ethyl acetate

2: Ag₂O / benzene / 48 h / Ambient temperature

3: Zn-powder / acetic acid / 3 h / 50 °C

4: dicyclohexylcarbodiimide, dimethylaminopyridine / CH₂Cl₂ / 12 h / Ambient temperature

5: 90percent acetic acid / 0.33 h / 90 °C

With dmap; acetic acid; triethylamine; dicyclohexyl-carbodiimide; silver(l) oxide; zinc; In dichloromethane; acetic acid; ethyl acetate; benzene;
DOI:10.1016/S0040-4039(00)81830-4

Reference yield:

: 100-39-0
benzyl bromide

: 87357-75-3
(R)-3-Benzyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-5-acetylamino-2-((2R,3R,4R,5S,6R)-3-acetylamino-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-6-allyloxy-4-((R)-3-benzyloxy-tetradecanoyloxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Ag₂O / benzene / 48 h / Ambient temperature

2: Zn-powder / acetic acid / 3 h / 50 °C

3: dicyclohexylcarbodiimide, dimethylaminopyridine / CH₂Cl₂ / 12 h / Ambient temperature

4: 90percent acetic acid / 0.33 h / 90 °C

With dmap; acetic acid; dicyclohexyl-carbodiimide; silver(l) oxide; zinc; In dichloromethane; acetic acid; benzene;
DOI:10.1016/S0040-4039(00)81830-4