2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside

Base Information

Chemical Name:2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside
CAS No.:105165-77-3
Molecular Formula:C₈₀H₇₇NO₁₄S₂
Molecular Weight:1340.62
Hs Code.:

2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside

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Chemical Property of 2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside

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Technology Process of 2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside

There total 3 articles about 2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105165-70-6
2-O-tosyl-6,1',6'-tri-O-tritylsucrose

: 105165-77-3
2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / sodium methoxide / methanol / 2 h / Heating

2: 1.) ammonium chloride, 2.) pyridine / 1.) 2-methoxyethanol, water, 100 deg C, 1.5 h 2.) r.t.

With pyridine; ammonium chloride; sodium methylate; In methanol;
DOI:10.1016/0008-6215(86)80005-2

Reference yield:

: 35674-14-7
1,6-di-O-trityl-β-D-fructofuranosyl 6-O-trityl-α-D-glucopyranoside

: 105165-77-3
2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / pyridine / Ambient temperature

2: 41 percent / sodium methoxide / methanol / 2 h / Heating

3: 1.) ammonium chloride, 2.) pyridine / 1.) 2-methoxyethanol, water, 100 deg C, 1.5 h 2.) r.t.

With pyridine; ammonium chloride; sodium methylate; In methanol;
DOI:10.1016/0008-6215(86)80005-2

Reference yield:

: 108-24-7
acetic anhydride

: 105165-72-8
2,3-anhydro-6-O-trityl-α-D-mannopyranosyl 1,6-di-O-trityl-β-D-fructofuranoside

: 128-04-1
sodium dimethyldithiocarbamate

: 105165-77-3
2,4-di-O-acetyl-3-S-(N,N-dimethylaminothiocarbonyl)-3-thio-6-O-trityl-α-D-altropyranosyl 3,4-di-O-acetyl-1,6-di-O-trityl-β-D-fructofuranoside

Guidance literature:: With pyridine; ammonium chloride; Yield given. Multistep reaction; 1.) 2-methoxyethanol, water, 100 deg C, 1.5 h 2.) r.t.;
DOI:10.1016/0008-6215(86)80005-2