2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone

Base Information

Chemical Name:2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone
CAS No.:115346-59-3
Molecular Formula:C₁₂H₂₂O₄
Molecular Weight:230.304
Hs Code.:

Synonyms:

Suppliers and Price of 2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone

There total 3 articles about 2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 5344-23-0
diethoxyacetaldehyde

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 115346-59-3,115346-61-7
2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) -60 deg C to room temperature, 2.) room temperature, 3 h;

Reference yield:

: 60468-85-1
acetoxyacetaldehyde diethylacetate

: 115346-59-3,115346-61-7
2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / LAH / diethyl ether / 0 °C

2: 1.) oxalyl chloride, DMSO, 2.) triethylamine / tetrahydrofuran / 1.) -30 deg C, 15 min, 2.) - 60 deg C --> room temperature, room temperature, 1 h

3: 35 percent / LDA / tetrahydrofuran / 1.) -60 deg C to room temperature, 2.) room temperature, 3 h

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;

Reference yield:

: 621-63-6
glycoaldehyde diethyl acetal

: 115346-59-3,115346-61-7
2-(2,2-diethoxy 1-hydroxy ethyl) cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl chloride, DMSO, 2.) triethylamine / tetrahydrofuran / 1.) -30 deg C, 15 min, 2.) - 60 deg C --> room temperature, room temperature, 1 h

2: 35 percent / LDA / tetrahydrofuran / 1.) -60 deg C to room temperature, 2.) room temperature, 3 h

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran;