{Cl₂(tetra-m-tolylporphyrinato)vanadium(IV)}

Base Information

Chemical Name:{Cl₂(tetra-m-tolylporphyrinato)vanadium(IV)}
CAS No.:83582-02-9
Molecular Formula:C₄₈H₃₆Cl₂N₄V
Molecular Weight:790.688
Hs Code.:

{Cl<sub>2</sub>(tetra-m-tolylporphyrinato)vanadium(IV)}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Cl₂(tetra-m-tolylporphyrinato)vanadium(IV)}

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Technology Process of {Cl₂(tetra-m-tolylporphyrinato)vanadium(IV)}

There total 2 articles about {Cl₂(tetra-m-tolylporphyrinato)vanadium(IV)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 79-37-8
oxalyl dichloride

: 86221-96-7
{(tetra-m-toylporphyrinato)(O)vanadium(IV)}

: 83582-02-9
{Cl₂(tetra-m-tolylporphyrinato)vanadium(IV)}

Guidance literature:: In dichloromethane; under Ar, V-compd. dissolved in CH2Cl2, 10 equiv of (COCl)2 added, maintained at room temp. with stirring for 12 h, placed in refrigerator; filtered, washed with hexane, dried; elem. anal.;
DOI:10.1039/DT9820001451

Reference yield: 78.0%

: 86221-96-7
{(tetra-m-toylporphyrinato)(O)vanadium(IV)}

: 83582-02-9
{Cl₂(tetra-m-tolylporphyrinato)vanadium(IV)}

Guidance literature:: With thionyl chloride; In toluene; under Ar, V-compd. dissolved in toluene, 8.2 equiv of SOCl2 added, maintained at room temp. with stirring for 24 h, placed in refrigerator; filtered, washed with hexane, dried; elem. anal.;
DOI:10.1039/DT9820001451

Reference yield: 42.0%

: 10544-50-0
sulfur

: 83582-02-9
{Cl₂(tetra-m-tolylporphyrinato)vanadium(IV)}

: 85976-53-0
{(tetra-m-toylporphyrinato)(S)vanadium(IV)}

Guidance literature:: With Zn#Hg; In tetrahydrofuran; (under Ar); stirring of the chloro-complex in THF with Zn#Hg yields the THF-complex for 24 h, addn. of sulphur after sepg. from the amalgame, stirring for 5 h at room temp.; evapn. of the solvent, sublimation, chromy., recrystn. (toluene-heptane), elem. anal.;