(2-phenylindenyl)2ZrMe₂

Base Information

Chemical Name:(2-phenylindenyl)2ZrMe₂
CAS No.:172414-52-7
Molecular Formula:C₃₂H₂₈Zr
Molecular Weight:503.798
Hs Code.:

Synonyms:

Suppliers and Price of (2-phenylindenyl)2ZrMe₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2-phenylindenyl)2ZrMe₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2-phenylindenyl)2ZrMe₂

There total 1 articles about (2-phenylindenyl)2ZrMe₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 4505-48-0
2-phenylindene

: 917-54-4
methyllithium

: 10026-11-6
zirconium(IV) chloride

: 172414-52-7
(2-phenylindenyl)2ZrMe₂

Guidance literature:: In diethyl ether; pentane; CH3Li/Et2O added dropwise to a soln. of 2-phenylindene in Et2O at -78°C, allowed to warm to room temp. and stirred in the dark for 12 h, added to a suspn. of ZrCl4 in pentane, reacted for 1 h; evapd. (vac.), dissolved in toluene, filtered, concd. (vac.), crystd. at-50°C;
DOI:10.1021/om050473k

Reference yield:

: 172414-52-7
(2-phenylindenyl)2ZrMe₂

: 1109-15-5
tris(pentafluorophenyl)borate

: 870558-70-6
[(2-phenylindenyl)2ZrMe][CH₃B(C₆F₅)3]

Guidance literature:: In ⁽²⁾H₈-toluene; (Schlenk or under Ar); Zr-complex, B(C6F5)3 and toluene-d8 mixed, loadedin NMR tube, reacted at ambient temp. for 15 min; monitored by NMR;
DOI:10.1016/j.jorganchem.2005.01.070