8,9,12-triiiodo-1,2-dicarba-closo-dodecaborane

Base Information

Chemical Name:8,9,12-triiiodo-1,2-dicarba-closo-dodecaborane
CAS No.:20313-41-1
Molecular Formula:C₂H₉B₁₀I₃
Molecular Weight:521.917
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8,9,12-triiiodo-1,2-dicarba-closo-dodecaborane

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Technology Process of 8,9,12-triiiodo-1,2-dicarba-closo-dodecaborane

There total 4 articles about 8,9,12-triiiodo-1,2-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 16872-09-6
1,2-dicarba-closo-dodecaborane⁽¹²⁾

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 29386-25-2
8,9-diiodo-1,2-dicarba-closo-dodecarborane⁽¹²⁾

: 17830-03-4
9-iodo-o-carborane

: 17702-35-1
9,12-diiodo-1,2-dicarba-closo-dodecarborane⁽¹²⁾

: 20313-41-1
8,9,12-triiiodo-1,2-dicarba-closo-dodecaborane

Guidance literature:: In neat (no solvent); (under N2); tube charged with B-compound and I2 under vac., cooled to liq. N2 temp., sealed, heated to 170°C for 30 min, maintained for 3.5 h, slowly cooled to room temp.; sublimed at 50°C under reduced pressure, recrystd. from hexane/CHCl3 6:1;
DOI:10.1021/ic800362z

Reference yield: 70.0%

: 16872-09-6
1,2-dicarba-closo-dodecaborane⁽¹²⁾

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 29386-25-2
8,9-diiodo-1,2-dicarba-closo-dodecarborane⁽¹²⁾

: 17702-35-1
9,12-diiodo-1,2-dicarba-closo-dodecarborane⁽¹²⁾

: 20313-41-1
8,9,12-triiiodo-1,2-dicarba-closo-dodecaborane

Guidance literature:: In neat (no solvent); (under N2); tube charged with B-compound and I2 under vac., cooled to liq. N2 temp., sealed, heated to 180°C for 30 min, maintained for 3.5 h, slowly cooled to room temp.; sublimed at 50°C under reduced pressure;
DOI:10.1021/ic800362z

Reference yield: 57.0%

: 16872-09-6
1,2-dicarba-closo-dodecaborane⁽¹²⁾

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 17702-35-1
9,12-diiodo-1,2-dicarba-closo-dodecarborane⁽¹²⁾

: 20313-41-1
8,9,12-triiiodo-1,2-dicarba-closo-dodecaborane

Guidance literature:: In neat (no solvent); (under N2); tube charged with B-compound and I2 under vac., cooled to liq. N2 temp., sealed, heated to 195°C for 30 min, maintained for 4.5 h, slowly cooled to room temp.; sublimed at 50°C under reduced pressure;
DOI:10.1021/ic800362z