[2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC₂B₉H₁₀]

Base Information

Chemical Name:[2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC₂B₉H₁₀]
CAS No.:1153642-34-2
Molecular Formula:C₁₀H₁₅B₉NO₃Tc
Molecular Weight:393.533
Hs Code.:

[2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC<sub>2</sub>B<sub>9</sub>H<sub>10</sub>]

Synonyms:

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Chemical Property of [2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC₂B₉H₁₀]

Chemical Property:

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Technology Process of [2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC₂B₉H₁₀]

There total 3 articles about [2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC₂B₉H₁₀] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1153642-28-4
Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅⁽⁹⁹⁾Tc(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅⁽⁹⁹⁾Tc(CO)3

: 7664-93-9
sulfuric acid

: 7632-00-0
sodium nitrite

: 1153642-34-2
[2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC₂B₉H₁₀]

Guidance literature:: In water; acetonitrile; addn. of NaNO2 to a soln. of Tc complex in acetonitrile, addn. of aq. H2SO4, react. for 5 min; C18 solid phase extn. cartridge, flushing with acetonitrile/H2O 1:1, elution with acetonitrile, identified by radio-HPLC (Nucleosil C18 column, 85-98% acetonitrile in H2O 0-17 min, 98% acetonitrile in H2O 17-20 min);
DOI:10.1021/om8011807

Reference yield:

: 1153642-28-4
Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅⁽⁹⁹⁾Tc(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅⁽⁹⁹⁾Tc(CO)3

: nitrosonium tetrafluoroborate

: 1153642-34-2
[2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC₂B₉H₁₀]

Guidance literature:: In not given; C18 solid phase extn. cartridge, flushing with H2O, elution with acetonitrile, identified by radio-HPLC (Nucleosil C18 column, 85-98% acetonitrile in H2O 0-17 min, 98% acetonitrile in H2O 17-20 min);
DOI:10.1021/om8011807

Reference yield:

: nitrosylsulfuric acid

: 1153642-28-4
Na⁽¹⁺⁾*C₂B₉H₁₀C₆H₅⁽⁹⁹⁾Tc(CO)3^(1-)=NaC₂B₉H₁₀C₆H₅⁽⁹⁹⁾Tc(CO)3

: 1153642-34-2
[2,2-(CO)2-2-(NO)-8-(Ph)-1,1,8-closo-(99m)TcC₂B₉H₁₀]

Guidance literature:: In not given; C18 solid phase extn. cartridge, flushing with H2O, elution with acetonitrile, identified by radio-HPLC (Nucleosil C18 column, 85-98% acetonitrile in H2O 0-17 min, 98% acetonitrile in H2O 17-20 min);
DOI:10.1021/om8011807