trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II)

Base Information

Chemical Name:trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II)
CAS No.:96857-75-9
Molecular Formula:C₃₈H₃₄Cl₄P₂Pd₂
Molecular Weight:907.287
Hs Code.:

Synonyms:

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Chemical Property of trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II)

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Technology Process of trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II)

There total 8 articles about trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: sodium tetrachloropalladate(II)

: 7650-91-1
benzyldiphenylphosphane

: 61046-58-0,55529-12-9,49607-83-2
dichlorobis[benzyldiphenylphosphine]palladium(II)

: 96857-75-9,96895-82-8
trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II)

Guidance literature:: With SiO₂; In neat (no solvent); under Ar, glove box; to PBnPh2 added Na2PdCl4, SiO2, stirred (1 min), 40°C, 1 h; washed from SiO2 (acetone), solid dissolved in CH2Cl2, TLC (SiO2, CH2Cl2); elem. anal., XRD;
DOI:10.1016/j.jorganchem.2011.06.026

Reference yield: 69.0%

: 3375-31-3
palladium diacetate

: 7650-91-1
benzyldiphenylphosphane

: 96857-75-9,96895-82-8
trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II)

Guidance literature:: With SiO₂; LiCl; In neat (no solvent); under Ar, glove box; to PBnPh2, Pd(OAc)2 and SiO2 added, 50°C, 72-168 h, washed from SiO2 (acetone), LiCl added, stirred overnight; solid dissolved in CH2Cl2, filtered, crystn. (CH2Cl2); elem. anal., XRD;
DOI:10.1016/j.jorganchem.2011.06.026

Reference yield: 68.0%

: sodium tetrachloropalladate(II)

: 7650-91-1
benzyldiphenylphosphane

: di-μ-chlorobis-[2-[(diphenylphosphino)methyl]phenyl-C,P]dipalladium(II)

: 61046-58-0,55529-12-9,49607-83-2
dichlorobis[benzyldiphenylphosphine]palladium(II)

: 96857-75-9,96895-82-8
trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II)

Guidance literature:: With SiO₂; In neat (no solvent); under Ar, glove box; to PBnPh2 added Na2PdCl4, SiO2, stirred (1 min), 85°C, 5 h; washed from SiO2 (acetone), solid dissolved in CH2Cl2, TLC (SiO2, CH2Cl2); elem. anal., XRD;
DOI:10.1016/j.jorganchem.2011.06.026