Technology Process of C14H19NO3
There total 4 articles about C14H19NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Carica papaya lipase;
In
hexane;
at 45 ℃;
for 40h;
Resolution of racemate;
Enzymatic reaction;
DOI:10.1002/ejoc.201201055
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide / water / 8 h / 40 °C / pH 11
2.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / Cooling with ice
2.2: 20 °C
3.1: Carica papaya lipase / hexane / 40 h / 45 °C / Resolution of racemate; Enzymatic reaction
With
benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide;
In
hexane; dichloromethane; water;
DOI:10.1002/ejoc.201201055
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ammonium acetate / ethanol / 12 h / Reflux
2.1: sodium hydroxide / water / 8 h / 40 °C / pH 11
3.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / Cooling with ice
3.2: 20 °C
4.1: Carica papaya lipase / hexane / 40 h / 45 °C / Resolution of racemate; Enzymatic reaction
With
ammonium acetate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide;
In
ethanol; hexane; dichloromethane; water;
DOI:10.1002/ejoc.201201055