{RhCl((C₆H₅)3P)((C₆H₅)2PO₂CCHCHCH₃)}

Base Information

Chemical Name:{RhCl((C₆H₅)3P)((C₆H₅)2PO₂CCHCHCH₃)}
CAS No.:128025-04-7
Molecular Formula:C₃₄H₃₀ClO₂P₂Rh
Molecular Weight:670.917
Hs Code.:

{RhCl((C<sub>6</sub>H<sub>5</sub>)3P)((C<sub>6</sub>H<sub>5</sub>)2PO<sub>2</sub>CCHCHCH<sub>3</sub>)}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {RhCl((C₆H₅)3P)((C₆H₅)2PO₂CCHCHCH₃)}

Chemical Property:

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Technology Process of {RhCl((C₆H₅)3P)((C₆H₅)2PO₂CCHCHCH₃)}

There total 1 articles about {RhCl((C₆H₅)3P)((C₆H₅)2PO₂CCHCHCH₃)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 14694-95-2
Wilkinson's catalyst

: 136529-59-4
Diphenylphosphino but-3-enoate

: 128025-04-7
{RhCl((C₆H₅)3P)((C₆H₅)2PO₂CCHCHCH₃)}

Guidance literature:: In tetrahydrofuran; under N2, 0°C; filtration, reduction of vol., addn. of light petroleum, recrystn. from CH2Cl2-diethyl ether, identified by (1)H- and (31)P-NMR spectra;
DOI:10.1039/DT9910001765

Reference yield: 73.0%

: 128025-04-7
{RhCl((C₆H₅)3P)((C₆H₅)2PO₂CCHCHCH₃)}

: 59471-15-7
potassium crotanoate

: 136776-57-3
but-2-enoato(diphenylphosphino but-2-enoate)(triphenylphosphine)rhodium(I)

Guidance literature:: In tetrahydrofuran; stirred for 2 h, filtered to eliminate the excess of K(O2CCHCHMe), evapd. under vac., light petroleum added, filtered off and dried under vac.; elem. anal.;
DOI:10.1039/DT9910001929

Reference yield:

: 128025-04-7
{RhCl((C₆H₅)3P)((C₆H₅)2PO₂CCHCHCH₃)}

: 50807-07-3
{NH(C₂H₅)3}⁽¹⁺⁾*{(CH₃)CHCHCO₂}^(1-)={NH(C₂H₅)3}{(CH₃)CHCHCO₂}

: 136776-57-3
but-2-enoato(diphenylphosphino but-2-enoate)(triphenylphosphine)rhodium(I)

Guidance literature:: In tetrahydrofuran; (NHEt3)(MeHCCHCO2) prepared in situ, stirred for 2 h, filtered to eliminate the excess of K(O2CCHCHMe), evapd. under vac., light petroleum added, filtered off and dried under vac.;
DOI:10.1039/DT9910001929