C₅₉H₇₀N₁₀O₁₃

Base Information

• Chemical Name: C₅₉H₇₀N₁₀O₁₃
• CAS No.: 1403678-01-2
• Molecular Formula: C₅₉H₇₀N₁₀O₁₃
• Molecular Weight: 1127.26
• Mol file: 1403678-01-2.mol

Synonyms:

Chemical Property of C₅₉H₇₀N₁₀O₁₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₇₀N₁₀O₁₃

There total 4 articles about C₅₉H₇₀N₁₀O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-(4-(azidomethyl)phenyl)ethene-1,1,2-triyl)tribenzene (1403677-99-5) + C32H49N7O13 (1403678-00-1) → C59H70N10O13 (1403678-01-2)

Guidance literature:

With L-ascorbic acid sodium salt; copper(II) sulfate; In water; dimethyl sulfoxide; at 20 ℃; for 24h;

DOI:10.1021/ja3064588

Reference yield:

Diphenylmethane (101-81-5) → C59H70N10O13 (1403678-01-2)

Guidance literature:

Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux

4.1: sodium azide / dimethyl sulfoxide / 20 °C / Inert atmosphere

5.1: L-ascorbic acid sodium salt; copper(II) sulfate / dimethyl sulfoxide; water / 24 h / 20 °C

With N-Bromosuccinimide; n-butyllithium; sodium azide; L-ascorbic acid sodium salt; toluene-4-sulfonic acid; copper(II) sulfate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; hexane; water; dimethyl sulfoxide; toluene;

DOI:10.1021/ja3064588

Reference yield:

4-Methylbenzophenone (134-84-9) → C59H70N10O13 (1403678-01-2)

Guidance literature:

Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux

4.1: sodium azide / dimethyl sulfoxide / 20 °C / Inert atmosphere

5.1: L-ascorbic acid sodium salt; copper(II) sulfate / dimethyl sulfoxide; water / 24 h / 20 °C

With N-Bromosuccinimide; n-butyllithium; sodium azide; L-ascorbic acid sodium salt; toluene-4-sulfonic acid; copper(II) sulfate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; hexane; water; dimethyl sulfoxide; toluene;

DOI:10.1021/ja3064588

upstream raw materials:

1-(4-methylphenyl)-1,2,2-triphenylethanol

(2-(4-(azidomethyl)phenyl)ethene-1,1,2-triyl)tribenzene

C₃₂H₄₉N₇O₁₃

Diphenylmethane