2-(2-{2-[2-tert-butoxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propylcarbamoyl)-succinic acid 4-tert-butyl ester 1-(4-nitro-benzyl) ester

Base Information

Chemical Name:2-(2-{2-[2-tert-butoxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propylcarbamoyl)-succinic acid 4-tert-butyl ester 1-(4-nitro-benzyl) ester
CAS No.:211689-77-9
Molecular Formula:C₅₀H₅₈N₆O₁₁
Molecular Weight:919.044
Hs Code.:

2-(2-{2-[2-<i>tert</i>-butoxycarbonylamino-3-(1<i>H</i>-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propylcarbamoyl)-succinic acid 4-<i>tert</i>-butyl ester 1-(4-nitro-benzyl) ester

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Chemical Property of 2-(2-{2-[2-tert-butoxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propylcarbamoyl)-succinic acid 4-tert-butyl ester 1-(4-nitro-benzyl) ester

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Technology Process of 2-(2-{2-[2-tert-butoxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propylcarbamoyl)-succinic acid 4-tert-butyl ester 1-(4-nitro-benzyl) ester

There total 2 articles about 2-(2-{2-[2-tert-butoxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propylcarbamoyl)-succinic acid 4-tert-butyl ester 1-(4-nitro-benzyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 211689-63-3
(2-{2-[2-tert-butoxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propyl)-carbamic acid benzyl ester

: 211689-77-9
2-(2-{2-[2-tert-butoxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propylcarbamoyl)-succinic acid 4-tert-butyl ester 1-(4-nitro-benzyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol; dimethylformamide

2: EDC*HCl; HOBt / dimethylformamide

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(01)00841-1

Reference yield:

: 211689-79-1
2-(4-Nitrobenzyloxycarbonyl)succinic acid 4-tert-butyl ester

: 211689-76-8
[1-[1-(1-aminomethyl-2-phenyl-ethylcarbamoyl)-2-phenyl-ethylcarbamoyl]-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

: 211689-77-9
2-(2-{2-[2-tert-butoxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propylcarbamoyl)-succinic acid 4-tert-butyl ester 1-(4-nitro-benzyl) ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(01)00841-1