N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

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Chemical Name:N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide
CAS No.:1315330-98-3
Molecular Formula:C₇₃H₇₉N₃O₈S
Molecular Weight:1158.51
Hs Code.:

N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

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Chemical Property of N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

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Technology Process of N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

There total 11 articles about N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1315330-95-0
3-[4-(4-aminophenyl)-5-methyl-thien-2-yl]-2-cyanoacrylic acid

: 1315330-97-2
N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide

: 1315330-98-3
N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

Guidance literature:: With 1H-imidazole; at 130 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.dyepig.2011.03.022

Reference yield:

: 23708-56-7
6-undecanol

: 1315330-98-3
N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

2: potassium hydroxide; tert-butyl alcohol / 1 h / 80 °C

3: 1H-imidazole / 2 h / 130 °C / Inert atmosphere

With 1H-imidazole; potassium carbonate; potassium hydroxide; tert-butyl alcohol; In N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2011.03.022

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1315330-98-3
N-(2,6-diisopropylphenyl)-N'-{4-[2-methyl-5-(cyanoacrylic acid)-3-thienyl]-phenyl}-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; bromine; iodine / 10 h / 85 °C

2: propionic acid / 26 h / 130 °C

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

4: potassium hydroxide; tert-butyl alcohol / 1 h / 80 °C

5: 1H-imidazole / 2 h / 130 °C / Inert atmosphere

With 1H-imidazole; sulfuric acid; bromine; iodine; potassium carbonate; propionic acid; potassium hydroxide; tert-butyl alcohol; In N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2011.03.022