N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide

Base Information

Chemical Name:N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide
CAS No.:1315330-97-2
Molecular Formula:C₅₈H₆₉NO₇
Molecular Weight:892.188
Hs Code.:

Synonyms:N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide

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Chemical Property of N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide

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Technology Process of N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide

There total 6 articles about N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1315330-96-1
N,N'-bis(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic diimide

: 1315330-97-2
N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide

Guidance literature:: With potassium hydroxide; tert-butyl alcohol; at 80 ℃; for 1h;
DOI:10.1016/j.dyepig.2011.03.022

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1315330-97-2
N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; bromine; iodine / 10 h / 85 °C

2: propionic acid / 26 h / 130 °C

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

4: potassium hydroxide; tert-butyl alcohol / 1 h / 80 °C

With sulfuric acid; bromine; iodine; potassium carbonate; propionic acid; potassium hydroxide; tert-butyl alcohol; In N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2011.03.022

Reference yield:

: 927-49-1
dipentyl ketone

: 1315330-97-2
N-(2,6-diisopropylphenyl)-1,7-bis(6-undecanoxy)perylene-3,4,9,10-tetracarboxylic 3,4-anhydride 9,10-imide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol / 1 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

3: potassium hydroxide; tert-butyl alcohol / 1 h / 80 °C

With sodium tetrahydroborate; potassium carbonate; potassium hydroxide; tert-butyl alcohol; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2011.03.022