bis(tricyclohexylposphane)copper(I) formate*formic acid

Base Information

Chemical Name:bis(tricyclohexylposphane)copper(I) formate*formic acid
CAS No.:1264715-54-9
Molecular Formula:CH₂O₂*C₃₇H₆₇CuO₂P₂
Molecular Weight:715.457
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(tricyclohexylposphane)copper(I) formate*formic acid

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Technology Process of bis(tricyclohexylposphane)copper(I) formate*formic acid

There total 1 articles about bis(tricyclohexylposphane)copper(I) formate*formic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 64-18-6
formic acid

: copper(I) formate

: 2622-14-2
tricyclohexylphosphine

: 1264715-54-9
bis(tricyclohexylposphane)copper(I) formate*formic acid

Guidance literature:: In dichloromethane; standard Schlenk techniques under N2;formic acid in CH2Cl2 dropwise added to Cu-compd. in CH2Cl2 at -20°C, stirred for 30 min at -20°C, P-compd. in CH2Cl2 (molar ratio Cu-compd.:P-compd.=1:2) dropwise added, stirred for 1 h at -20°C; filtered through a pad of Celite, all volatiles removed in vac., crystallized from CH2Cl2 at -20°C, elem. anal.;
DOI:10.1016/j.ica.2010.05.048