C₂₂H₁₈N₂O₃

Base Information

Chemical Name:C₂₂H₁₈N₂O₃
CAS No.:1396795-82-6
Molecular Formula:C₂₂H₁₈N₂O₃
Molecular Weight:358.397
Hs Code.:

C<sub>22</sub>H<sub>18</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₈N₂O₃

Chemical Property:

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Technology Process of C₂₂H₁₈N₂O₃

There total 4 articles about C₂₂H₁₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21419-74-9
2-nitro-3-hydroxybiphenyl

: 1396795-82-6
C₂₂H₁₈N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 20 °C

2: tetrahydrofuran / 2 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C / Cooling with ice

4: hydrogenchloride / acetic acid; 1,4-dioxane / 4 h / 50 °C

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; 1,4-dioxane; methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.07.023

Reference yield:

: 109877-38-5
2-amino-3-hydroxybiphenyl

: 1396795-82-6
C₂₂H₁₈N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 2 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C / Cooling with ice

3: hydrogenchloride / acetic acid; 1,4-dioxane / 4 h / 50 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

With hydrogenchloride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; 1,4-dioxane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.07.023

Reference yield:

: 1396795-79-1
4-phenyl-1,3-benzoxazol-2(3H)-one

: 1396795-82-6
C₂₂H₁₈N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C / Cooling with ice

2: hydrogenchloride / acetic acid; 1,4-dioxane / 4 h / 50 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

With hydrogenchloride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.07.023