(+/-)-2-tert-butyl-3-phenyl-1-propyl acrylate

Base Information

Chemical Name:(+/-)-2-tert-butyl-3-phenyl-1-propyl acrylate
CAS No.:120390-60-5
Molecular Formula:C₁₆H₂₂O₂
Molecular Weight:246.349
Hs Code.:

Synonyms:

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Chemical Property of (+/-)-2-tert-butyl-3-phenyl-1-propyl acrylate

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Technology Process of (+/-)-2-tert-butyl-3-phenyl-1-propyl acrylate

There total 4 articles about (+/-)-2-tert-butyl-3-phenyl-1-propyl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 57985-62-3
(+/-)-2-tert-butyl-3-phenyl-1-propanol

: 79-10-7
acrylic acid

: 120390-60-5
(+/-)-2-tert-butyl-3-phenyl-1-propyl acrylate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 12h; Ambient temperature;

Reference yield:

: 1070-83-3
tert-Butylacetic acid

: 120390-60-5
(+/-)-2-tert-butyl-3-phenyl-1-propyl acrylate

Guidance literature:: Multi-step reaction with 3 steps

2: 80 percent / LAH / tetrahydrofuran / reflux, 1 h, RT, 36 h

3: 62 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 12 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 53483-12-8,110577-67-8
3,3-dimethyl-2-(phenylmethyl)butanoic acid

: 120390-60-5
(+/-)-2-tert-butyl-3-phenyl-1-propyl acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / LAH / tetrahydrofuran / reflux, 1 h, RT, 36 h

2: 62 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 12 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;