2,11-bis({5-methyl-2-(2-methoxy)ethoxy}phenyl)-6,7-dioxo-3,4:9,10-dibenzo-1,5,8,12-tetraazacyclotetradeca-1,3,9,11-tetraene-(-2)-N⁽¹⁾,N⁽⁵⁾,N⁽⁸⁾,N⁽¹²⁾-nickel(II)

Base Information

• Chemical Name: 2,11-bis({5-methyl-2-(2-methoxy)ethoxy}phenyl)-6,7-dioxo-3,4:9,10-dibenzo-1,5,8,12-tetraazacyclotetradeca-1,3,9,11-tetraene-(-2)-N⁽¹⁾,N⁽⁵⁾,N⁽⁸⁾,N⁽¹²⁾-nickel(II)
• CAS No.: 114287-50-2
• Molecular Formula: C₃₈H₃₈N₄NiO₆
• Molecular Weight: 705.433

Synonyms:

Chemical Property of 2,11-bis({5-methyl-2-(2-methoxy)ethoxy}phenyl)-6,7-dioxo-3,4:9,10-dibenzo-1,5,8,12-tetraazacyclotetradeca-1,3,9,11-tetraene-(-2)-N⁽¹⁾,N⁽⁵⁾,N⁽⁸⁾,N⁽¹²⁾-nickel(II)

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Technology Process of 2,11-bis({5-methyl-2-(2-methoxy)ethoxy}phenyl)-6,7-dioxo-3,4:9,10-dibenzo-1,5,8,12-tetraazacyclotetradeca-1,3,9,11-tetraene-(-2)-N⁽¹⁾,N⁽⁵⁾,N⁽⁸⁾,N⁽¹²⁾-nickel(II)

There total 1 articles about 2,11-bis({5-methyl-2-(2-methoxy)ethoxy}phenyl)-6,7-dioxo-3,4:9,10-dibenzo-1,5,8,12-tetraazacyclotetradeca-1,3,9,11-tetraene-(-2)-N⁽¹⁾,N⁽⁵⁾,N⁽⁸⁾,N⁽¹²⁾-nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

nickel(II) nitrate hexahydrate + sodium methylate (124-41-4) + N,N'-Bisphenyl>oxamide (114316-63-1) + 1,2-diaminoethane dihydrochloride (333-18-6) → 2,11-bis({5-methyl-2-(2-methoxy)ethoxy}phenyl)-6,7-dioxo-3,4:9,10-dibenzo-1,5,8,12-tetraazacyclotetradeca-1,3,9,11-tetraene-(-2)-N(1),N(5),N(8),N(12)-nickel(II) (114287-50-2)

Guidance literature:

In methanol; To a suspension of the oxalamide in abs. MeOH was given Ni(NO3)2*6H2O and H2NCH2CH2NH2*2HCl in CH3ONa soln.; the mixture was stirred at 55°C.; The two isomers were separated by preparative TCL (SiO2, CHCl3-(CH3)2CO (6:1)).;

upstream raw materials:

sodium methylate

N,N'-Bisphenyl>oxamide

1,2-diaminoethane dihydrochloride

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