[(HC(CMeN(C6H3-i-Pr2-2,6)2)2)Al(μ-S)2Sn(μ-S)2Al(HC(CMeN(C6H3-i-Pr2-2,6)2)2)]

Base Information

• Chemical Name: [(HC(CMeN(C6H3-i-Pr2-2,6)2)2)Al(μ-S)2Sn(μ-S)2Al(HC(CMeN(C6H3-i-Pr2-2,6)2)2)]
• CAS No.: 886058-60-2
• Molecular Formula: C₅₈H₈₂Al₂N₄S₄Sn
• Molecular Weight: 1136.25

Synonyms:

Chemical Property of [(HC(CMeN(C6H3-i-Pr2-2,6)2)2)Al(μ-S)2Sn(μ-S)2Al(HC(CMeN(C6H3-i-Pr2-2,6)2)2)]

Chemical Property:

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Safty Information:

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Technology Process of [(HC(CMeN(C6H3-i-Pr2-2,6)2)2)Al(μ-S)2Sn(μ-S)2Al(HC(CMeN(C6H3-i-Pr2-2,6)2)2)]

There total 2 articles about [(HC(CMeN(C6H3-i-Pr2-2,6)2)2)Al(μ-S)2Sn(μ-S)2Al(HC(CMeN(C6H3-i-Pr2-2,6)2)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

SnCl4*2THF + [(((N(C6H3(CH(CH3)2)2)C(CH3))2CH)Al(SLi)2(tetrahydrofuran)2)2] → [(HC(CMeN(C6H3-i-Pr2-2,6)2)2)Al(μ-S)2Sn(μ-S)2Al(HC(CMeN(C6H3-i-Pr2-2,6)2)2)] (886058-60-2)

Guidance literature:

In toluene; (N2, Schlenk) SnCl4*2THF and Al-complex were mixed as solids in a flask,placed in liquid N2, toluene was added slowly, the mixt. was allowed to warm to ambient temp., stirred overnight; filtered, volatiles were removed in vac., the residue was washed with hexane; elem. anal.;

DOI:10.1021/ic052139m

Reference yield: 85.0%

[(((N(C6H3(CH(CH3)2)2)C(CH3))2CH)Al(SLi)2(tetrahydrofuran)2)2] + tin(IV) chloride (7646-78-8) → [(HC(CMeN(C6H3-i-Pr2-2,6)2)2)Al(μ-S)2Sn(μ-S)2Al(HC(CMeN(C6H3-i-Pr2-2,6)2)2)] (886058-60-2)

Guidance literature:

In tetrahydrofuran; (N2, Schlenk) SnCl4 was added dropwise to a soln. of complex in THF at -30°C, the mixt. was allowed to warm to room temp.; the solvent was removed in vac., extd. with toluene, kept at room temp. for 2 days;

DOI:10.1021/ic052139m

upstream raw materials:

tin(IV) chloride

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