3-Acetyl-3-phenylhexanedioic Acid 1-Dimethylamide 6-Ethyl Ester

Base Information

Chemical Name:3-Acetyl-3-phenylhexanedioic Acid 1-Dimethylamide 6-Ethyl Ester
CAS No.:74528-59-9
Molecular Formula:C₁₈H₂₅NO₄
Molecular Weight:319.401
Hs Code.:

Synonyms:

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Chemical Property of 3-Acetyl-3-phenylhexanedioic Acid 1-Dimethylamide 6-Ethyl Ester

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Technology Process of 3-Acetyl-3-phenylhexanedioic Acid 1-Dimethylamide 6-Ethyl Ester

There total 3 articles about 3-Acetyl-3-phenylhexanedioic Acid 1-Dimethylamide 6-Ethyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 64-17-5
ethanol

: 74528-42-0
3-(2-carboxyethyl)-3-phenyl-N,N-dimethyl-4-oxopentanamide

: 74528-59-9
3-Acetyl-3-phenylhexanedioic Acid 1-Dimethylamide 6-Ethyl Ester

Guidance literature:: With sulfuric acid; for 5h; Heating;
DOI:10.1055/s-1980-29034

Reference yield:

: 57734-28-8
3-Phenyllevulinic Acid Dimethylamide

: 74528-59-9
3-Acetyl-3-phenylhexanedioic Acid 1-Dimethylamide 6-Ethyl Ester

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / tetramethylammonium hydroxide / MeOH / 2-methyl-propan-2-ol / 2 h / 50 °C

2: 73 percent / 65percent H₂SO₄ / 1 h / 80 °C

3: 74 percent / H₂SO₄ / 5 h / Heating

With methanol; sulfuric acid; tetramethyl ammoniumhydroxide; In tert-butyl alcohol;
DOI:10.1055/s-1980-29034

Reference yield:

: 74528-36-2
3-Acetyl-5-cyano-3-phenyl-pentanoic acid dimethylamide

: 74528-59-9
3-Acetyl-3-phenylhexanedioic Acid 1-Dimethylamide 6-Ethyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 65percent H₂SO₄ / 1 h / 80 °C

2: 74 percent / H₂SO₄ / 5 h / Heating

With sulfuric acid;
DOI:10.1055/s-1980-29034