[Ir2Cl(CO)2(μ-dimethyl acetylenedicarboxylate)(bis(diphenylphosphino)methane)2]BF4

Base Information

Chemical Name:[Ir2Cl(CO)2(μ-dimethyl acetylenedicarboxylate)(bis(diphenylphosphino)methane)2]BF4
CAS No.:92270-21-8
Molecular Formula:BF₄*C₅₈H₅₀ClIr₂O₆P₄
Molecular Weight:1473.62
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ir2Cl(CO)2(μ-dimethyl acetylenedicarboxylate)(bis(diphenylphosphino)methane)2]BF4

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Technology Process of [Ir2Cl(CO)2(μ-dimethyl acetylenedicarboxylate)(bis(diphenylphosphino)methane)2]BF4

There total 3 articles about [Ir2Cl(CO)2(μ-dimethyl acetylenedicarboxylate)(bis(diphenylphosphino)methane)2]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 14104-20-2
silver tetrafluoroborate

: 92270-14-9
[Ir2(CO)2Cl2(μ-H3CO2CC=CCO2CH3)(bis(diphenylphosphino)methane)2]*CH2Cl2

: 92270-21-8
[Ir2Cl(CO)2(μ-dimethyl acetylenedicarboxylate)(bis(diphenylphosphino)methane)2]BF4

Guidance literature:: In tetrahydrofuran; byproducts: AgCl; To a soln. of complex in THF was added dropwise a soln. of AgBF4 in THF(N2 atm.);; Et2O was added, solid was collected and dried under N2 stream, redissolved in CH2Cl2 and filtered under N2, Et2O was added; elem. anal.;;