C₄₂H₆₂N₄O₅Si

Base Information

Chemical Name:C₄₂H₆₂N₄O₅Si
CAS No.:1289178-52-4
Molecular Formula:C₄₂H₆₂N₄O₅Si
Molecular Weight:731.064
Hs Code.:

C<sub>42</sub>H<sub>62</sub>N<sub>4</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₄₂H₆₂N₄O₅Si

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Technology Process of C₄₂H₆₂N₄O₅Si

There total 5 articles about C₄₂H₆₂N₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 344436-13-1
N-1,1'-biphenyl-2-yl-N'-4-piperidinylurea

: 1289178-52-4
C₄₂H₆₂N₄O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 50 °C

2: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

3: sodium tris(acetoxy)borohydride / methanol; dichloromethane

With sulfur trioxide pyridine complex; sodium tris(acetoxy)borohydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.043

Reference yield:

: 743459-97-4
N-1,1'-biphenyl-2-yl-N'-4-[1-(9-hydroxynonyl)]piperidinylurea

: 1289178-52-4
C₄₂H₆₂N₄O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

2: sodium tris(acetoxy)borohydride / methanol; dichloromethane

With sulfur trioxide pyridine complex; sodium tris(acetoxy)borohydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.01.043

Reference yield:

: 344436-12-0
N-1,1'-biphenyl-2-yl-N'-4-(1-benzyl)piperidinylurea

: 1289178-52-4
C₄₂H₆₂N₄O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1: 10% palladium on activated charcoal; ammonium bicarbonate / ethanol / 40 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 50 °C

3: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

4: sodium tris(acetoxy)borohydride / methanol; dichloromethane

With 10% palladium on activated charcoal; sulfur trioxide pyridine complex; sodium tris(acetoxy)borohydride; ammonium bicarbonate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.043