bis(4-fluorophenyl)methyl(1H-1,2,4-triazol-1-yl-methyl)germane

Base Information

Chemical Name:bis(4-fluorophenyl)methyl(1H-1,2,4-triazol-1-yl-methyl)germane
CAS No.:145066-05-3
Molecular Formula:C₁₆H₁₅F₂GeN₃
Molecular Weight:359.902
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(4-fluorophenyl)methyl(1H-1,2,4-triazol-1-yl-methyl)germane

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Technology Process of bis(4-fluorophenyl)methyl(1H-1,2,4-triazol-1-yl-methyl)germane

There total 1 articles about bis(4-fluorophenyl)methyl(1H-1,2,4-triazol-1-yl-methyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 145066-08-6
bis(4-fluorophenyl)(iodomethyl)methylgermane

: 41253-21-8
sodium triazole

: 145066-05-3
bis(4-fluorophenyl)methyl(1H-1,2,4-triazol-1-yl-methyl)germane

Guidance literature:: In N,N-dimethyl-formamide; byproducts: NaI; stirring mixt. of (FC6H4)2Ge(CH3)(CH2I) (5.73 mmol) and 1,2,4-triazole sodium salt (6.04 mmol) in DMF at 90°C for 3 h; cooling slurry to room temp., dilg. with H2O;; extg. with ether (3 x), washing combined exts. with satd. aq. NaCl-soln.; drying over anhydrous Na2SO4; removing solvent (reduced pressure); Kugelrohr distn. (170°C/0.1 torr); crystn. from (C2H5)2O/petroleum ether at -20°C; elem. anal.;;
DOI:10.1016/0022-328X(92)88005-4