Technology Process of C23H23NO4
There total 4 articles about C23H23NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3,4-bis(benzyloxy)benzoic acid;
With
diphenyl phosphoryl azide; triethylamine;
In
1,4-dioxane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
ethanol;
In
1,4-dioxane;
for 2h;
Reflux;
Inert atmosphere;
DOI:10.1007/s12272-011-0703-1
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / Inert atmosphere
2.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; acetonitrile; tert-butyl alcohol / 0.17 h / 20 °C / Inert atmosphere
3.1: diphenyl phosphoryl azide; triethylamine / 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere
3.2: 2 h / Reflux; Inert atmosphere
With
sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; potassium carbonate; triethylamine; potassium iodide;
In
1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
3.1: Curtius rearrangement / 3.2: Curtius rearrangement;
DOI:10.1007/s12272-011-0703-1
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / Inert atmosphere
2.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; acetonitrile; tert-butyl alcohol / 0.17 h / 20 °C / Inert atmosphere
3.1: diphenyl phosphoryl azide; triethylamine / 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere
3.2: 2 h / Reflux; Inert atmosphere
With
sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; potassium carbonate; triethylamine; potassium iodide;
In
1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
3.1: Curtius rearrangement / 3.2: Curtius rearrangement;
DOI:10.1007/s12272-011-0703-1
