(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OSiMe₃

Base Information

Chemical Name:(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OSiMe₃
CAS No.:1185739-16-5
Molecular Formula:C₄₃H₇₉FGeN₄OSi
Molecular Weight:787.8
Hs Code.:

(2,6-[CH<sub>2</sub>N(iPr)2]2C<sub>6</sub>H<sub>3</sub>)2Ge(F)OSiMe<sub>3</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OSiMe₃

Chemical Property:

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Technology Process of (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OSiMe₃

There total 3 articles about (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OSiMe₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 75-77-4
chloro-trimethyl-silane

: 1185739-14-3
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OH

: 594-19-4
tert.-butyl lithium

: 1185739-16-5
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OSiMe₃

Guidance literature:: In diethyl ether; under inert atm. soln. t-BuLi in pentane was added at 0°C to soln. Ge complex in Et2O and stirred for 30 min, Me3SiCl in Et2O was added, warmed to room temp.; pentane was added, soln. was filtered through Celite and evapd. in vacuo;
DOI:10.1002/ejic.200800494

Reference yield:

: 2,6-bis(diisopropylaminomethyl)phenyllithium

: 1185739-16-5
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OSiMe₃

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran

2: toluene

3: diethyl ether

In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1002/ejic.200800494

Reference yield:

: 1185739-13-2
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2

: 1185739-16-5
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OSiMe₃

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: diethyl ether

In diethyl ether; toluene;
DOI:10.1002/ejic.200800494