Ti(acetylacetonato)₂Cl₂

Base Information

• Chemical Name: Ti(acetylacetonato)₂Cl₂
• CAS No.: 16986-94-0
• Molecular Formula: C₁₀H₁₄Cl₂O₄Ti
• Molecular Weight: 317.005
• Mol file: 16986-94-0.mol

Synonyms:

Chemical Property of Ti(acetylacetonato)₂Cl₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ti(acetylacetonato)₂Cl₂

There total 3 articles about Ti(acetylacetonato)₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

titanium(IV) oxide bis(2,4-pentanedionate) + titanium tetrachloride (7550-45-0) → titanium(IV) oxychloride + Ti(acetylacetonato)2Cl2 (16986-94-0)

Guidance literature:

In 1,2-dichloro-ethane; for 2h; Schlenk technique; Reflux; Inert atmosphere;

DOI:10.1039/c3dt51378e

Reference yield: 79.0%

bis(acetylacetonate)oxidovanadium(IV) + titanium tetrachloride (7550-45-0) → vanadium(IV) chloride + Ti(acetylacetonato)2Cl2 (16986-94-0)

Guidance literature:

In n-heptane; 1,2-dichloro-ethane; for 2h; Schlenk technique; Inert atmosphere; Reflux;

DOI:10.1039/c3dt51378e

Reference yield:

titanium tetrachloride (7550-45-0) + acetylacetone (123-54-6,81235-32-7) → Ti(acetylacetonato)2Cl2 (16986-94-0)

Guidance literature:

In toluene; TiCl4 added under N2 to 1:3 mol excess of pentane-2,4-dione in sodium-dried toluene; heated under reflux for 20 min; solvent removed under reduced pressure; crystals grown by slow evapn. of soln. in toluene;

DOI:10.1107/S0108270100019181

upstream raw materials:

titanium tetrachloride

acetylacetone