Technology Process of [copper(I) bromide (η1-S-benzophenone thiosemicarbazone)(triphenylphosphine)2]*acetonitrile
There total 1 articles about [copper(I) bromide (η1-S-benzophenone thiosemicarbazone)(triphenylphosphine)2]*acetonitrile which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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In
acetonitrile;
to a soln. of CuBr in dry acetonitrile added solid benzophenone thiosemicarbazone; stirred for 3 h at room temp.; formed yellow solid separated;to this solid suspended in acetonitrile PPh3 added; stirring continued for further 1 h; refluxing 10 min; soln. filtered; allowed to evaporate at room temp.; elem. anal.;
DOI:10.1016/j.poly.2006.04.006
