Technology Process of C41H42N8O9S
There total 12 articles about C41H42N8O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 11 steps
1: sodium hydroxide / methanol; water / 0.17 h / Reflux
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C
4: triethylamine / dichloromethane / 1 h / 0 °C
5: potassium iodide / N,N-dimethyl-formamide / 20 °C
6: hydrazine hydrate / ethanol / 1 h / Reflux
7: ethyl acetate / 2 h / 50 °C
8: potassium phosphate / dichloromethane; water / 1 h / 22 °C
9: potassium phosphate; dipotassium peroxodisulfate / acetonitrile; water / 1.5 h / 75 °C
10: trifluoroacetic acid / 3 h / 0 °C
11: tetrahydrofuran / 15 h / 20 °C
With
potassium phosphate; dipotassium peroxodisulfate; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid; potassium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm400560z
- Guidance literature:
-
Multi-step reaction with 11 steps
1: sodium hydroxide / methanol; water / 0.17 h / Reflux
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C
4: triethylamine / dichloromethane / 1 h / 0 °C
5: potassium iodide / N,N-dimethyl-formamide / 20 °C
6: hydrazine hydrate / ethanol / 1 h / Reflux
7: ethyl acetate / 2 h / 50 °C
8: potassium phosphate / dichloromethane; water / 1 h / 22 °C
9: potassium phosphate; dipotassium peroxodisulfate / acetonitrile; water / 1.5 h / 75 °C
10: trifluoroacetic acid / 3 h / 0 °C
11: tetrahydrofuran / 15 h / 20 °C
With
potassium phosphate; dipotassium peroxodisulfate; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid; potassium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm400560z