P(S)S_P(O)>-(-)-bis(t-butylphenyl)thiophosphinate

Base Information

Chemical Name:P(S)S_P(O)>-(-)-bis(t-butylphenyl)thiophosphinate
CAS No.:128053-09-8
Molecular Formula:C₂₀H₂₈O₂P₂S
Molecular Weight:394.455
Hs Code.:

<R<sub>P(S)</sub>S<sub>P(O)</sub>>-(-)-bis(t-butylphenyl)thiophosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of P(S)S_P(O)>-(-)-bis(t-butylphenyl)thiophosphinate

Chemical Property:

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Technology Process of P(S)S_P(O)>-(-)-bis(t-butylphenyl)thiophosphinate

There total 4 articles about P(S)S_P(O)>-(-)-bis(t-butylphenyl)thiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54100-47-9
(R_p)-(+)-tert-Butylphenylphosphinothioic acid

: 128014-10-8
(R)-(+)-t-butyl(phenyl)phosphinic bromide

: 128053-09-8
P(S)S_P(O)>-(-)-bis(t-butylphenyl)thiophosphinate

Guidance literature:: With triethylamine; In dichloromethane; at 40 ℃; for 24h; other solvent benzene;

Reference yield:

: 6057-79-0,57956-51-1,82945-11-7
(S)-(-)-t-butyl(phenyl)phosphine oxide

: 128053-09-8
P(S)S_P(O)>-(-)-bis(t-butylphenyl)thiophosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / N-bromosuccinimide / CCl₄ / 1 h / 0 °C

2: triethylamine / CH₂Cl₂ / 24 h / 40 °C / other solvent benzene

With N-Bromosuccinimide; triethylamine; In tetrachloromethane; dichloromethane;

Reference yield:

: 51584-30-6
(S)-(-)-S-methyl tert-butylphenylphosphinothiolate

: 128053-09-8
P(S)S_P(O)>-(-)-bis(t-butylphenyl)thiophosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / bromine / CH₂Cl₂ / time: 6 months

2: triethylamine / CH₂Cl₂ / 24 h / 40 °C / other solvent benzene

With bromine; triethylamine; In dichloromethane;