C₂₅H₂₅ClF₃N₅O₃

Base Information

Chemical Name:C₂₅H₂₅ClF₃N₅O₃
CAS No.:1217506-27-8
Molecular Formula:C₂₅H₂₅ClF₃N₅O₃
Molecular Weight:535.953
Hs Code.:

C<sub>25</sub>H<sub>25</sub>ClF<sub>3</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₅H₂₅ClF₃N₅O₃

Chemical Property:

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Pictogram(s):
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Technology Process of C₂₅H₂₅ClF₃N₅O₃

There total 11 articles about C₂₅H₂₅ClF₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4389-45-1
3-methylantranilic acid

: 1217506-27-8
C₂₅H₂₅ClF₃N₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / Reflux

2: tetrahydrofuran / 20 °C / Cooling with ice

3: triethylamine / tetrahydrofuran / 8 h / 20 °C

With thionyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1002/cjoc.201200362

Reference yield:

: 22841-92-5
(3-chloro-2-pyridyl)hydrazine

: 1217506-27-8
C₂₅H₂₅ClF₃N₅O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium; ethanol / 0.17 h / Reflux

1.2: Reflux

2.1: dipotassium peroxodisulfate; sulfuric acid / acetonitrile / 4.5 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 100 °C

4.1: sodium hydroxide / water; methanol / 6 h / 20 °C

5.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C

6.1: triethylamine / tetrahydrofuran / 8 h / 20 °C

With dipotassium peroxodisulfate; oxalyl dichloride; ethanol; sulfuric acid; sodium; potassium carbonate; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cjoc.201200362

Reference yield:

: 2402-77-9
2,3-dichloro-pyridine

: 1217506-27-8
C₂₅H₂₅ClF₃N₅O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrazine hydrate / ethanol / 36 h / Reflux

2.1: sodium; ethanol / 0.17 h / Reflux

2.2: Reflux

3.1: dipotassium peroxodisulfate; sulfuric acid / acetonitrile / 4.5 h / Reflux

4.1: potassium carbonate / N,N-dimethyl-formamide / 100 °C

5.1: sodium hydroxide / water; methanol / 6 h / 20 °C

6.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C

7.1: triethylamine / tetrahydrofuran / 8 h / 20 °C

With dipotassium peroxodisulfate; oxalyl dichloride; ethanol; sulfuric acid; sodium; potassium carbonate; hydrazine hydrate; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cjoc.201200362