2,6-diisopropylphenylimino-2,2,6,6-tetramethylpiperidino-borane gallium trichloride

Base Information

• Chemical Name: 2,6-diisopropylphenylimino-2,2,6,6-tetramethylpiperidino-borane gallium trichloride
• CAS No.: 811804-20-3
• Molecular Formula: C₂₁H₃₅BCl₃GaN₂
• Molecular Weight: 502.415
• Mol file: 811804-20-3.mol

Synonyms:

Chemical Property of 2,6-diisopropylphenylimino-2,2,6,6-tetramethylpiperidino-borane gallium trichloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-diisopropylphenylimino-2,2,6,6-tetramethylpiperidino-borane gallium trichloride

There total 1 articles about 2,6-diisopropylphenylimino-2,2,6,6-tetramethylpiperidino-borane gallium trichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(2,6-diisopropylphenylimino)(2,2,6,6-tetramethylpiperidino)borane (113748-54-2) + Gallium trichloride (13450-90-3) → 2,6-diisopropylphenylimino-2,2,6,6-tetramethylpiperidino-borane gallium trichloride (811804-20-3)

Guidance literature:

In hexane; under anhydrous conditions, 20 % excess of B-compd. in hexane was added to hexane suspn. of metal-compd. at -50 °C, suspn. was slowly attain room temp.; elem. anal.;

DOI:10.1515/znb-2004-0608

Reference yield:

2,6-diisopropylphenylimino-2,2,6,6-tetramethylpiperidino-borane gallium trichloride (811804-20-3) → CH2(CH2C(CH3)2)2NBClN(C6H3(CH(CH3)2)2)GaCl2

Guidance literature:

anhydrous and mild conditions up to melting points of the compound;

DOI:10.1515/znb-2004-0608

upstream raw materials:

(2,6-diisopropylphenylimino)(2,2,6,6-tetramethylpiperidino)borane

Gallium trichloride