C₃₈H₄₇N₅O₅S*C₂HF₃O₂

Base Information

Chemical Name:C₃₈H₄₇N₅O₅S*C₂HF₃O₂
CAS No.:1422251-93-1
Molecular Formula:C₂HF₃O₂*C₃₈H₄₇N₅O₅S
Molecular Weight:799.912
Hs Code.:

C<sub>38</sub>H<sub>47</sub>N<sub>5</sub>O<sub>5</sub>S*C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>

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Chemical Property of C₃₈H₄₇N₅O₅S*C₂HF₃O₂

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Technology Process of C₃₈H₄₇N₅O₅S*C₂HF₃O₂

There total 6 articles about C₃₈H₄₇N₅O₅S*C₂HF₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3984-14-3
N,N-dimethylsulfamide

: C₃₆H₄₁N₃O₄

: 76-05-1
trifluoroacetic acid

: 1422251-93-1
C₃₈H₄₇N₅O₅S*C₂HF₃O₂

Guidance literature:: C₃₆H₄₁N₃O₄; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 50 ℃; for 1h; Inert atmosphere;

N,N-dimethylsulfamide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 125 ℃; for 1h; Sealed tube;

trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1139/cjc-2012-0319

Reference yield:

: C₂₂H₂₉NO₄

: 1422251-93-1
C₃₈H₄₇N₅O₅S*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridinium tribromide / tetrahydrofuran; chloroform / 0 - 20 °C

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; trifuran-2-yl-phosphane; potassium phosphate / water; 1,2-dimethoxyethane / 85 °C / Inert atmosphere

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dimethyl sulfoxide / 20 °C / Inert atmosphere

4.2: 50 °C / pH 4 - 5

5.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

5.2: 1 h / 125 °C / Sealed tube

With hydrogenchloride; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; pyridinium tribromide; trifuran-2-yl-phosphane; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; chloroform; water; dimethyl sulfoxide; 2.1: |Suzuki-Miyaura Coupling;
DOI:10.1139/cjc-2012-0319

Reference yield:

: 774213-79-5
methyl 2-bromo-1-(2-tert-butoxy-2-oxoethyl)-3-cyclohexyl-1H-indole-6-carboxylate

: 1422251-93-1
C₃₈H₄₇N₅O₅S*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; trifuran-2-yl-phosphane; potassium phosphate / water; 1,2-dimethoxyethane / 85 °C / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dimethyl sulfoxide / 20 °C / Inert atmosphere

3.2: 50 °C / pH 4 - 5

4.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

4.2: 1 h / 125 °C / Sealed tube

With hydrogenchloride; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium phosphate; trifuran-2-yl-phosphane; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; dimethyl sulfoxide; 1.1: |Suzuki-Miyaura Coupling;
DOI:10.1139/cjc-2012-0319