Technology Process of C19H20FNO
There total 6 articles about C19H20FNO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/chem.201203817
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 5,15,10,20-tetraphenylporphyrin; acetic anhydride / Inert atmosphere
2.1: ammonium acetate / acetic acid / 110 °C / Inert atmosphere
2.2: 48 h / 110 °C / Inert atmosphere
3.1: n-butyllithium; diisopropylamine / hexane; tetrahydrofuran / 2 h / -40 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
With
n-butyllithium; ammonium acetate; 5,15,10,20-tetraphenylporphyrin; acetic anhydride; diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane; acetic acid;
2.1: |Kroehnke Pyridine Synthesis / 2.2: |Kroehnke Pyridine Synthesis;
DOI:10.1002/chem.201203817
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium acetate / acetic acid / 110 °C / Inert atmosphere
1.2: 48 h / 110 °C / Inert atmosphere
2.1: n-butyllithium; diisopropylamine / hexane; tetrahydrofuran / 2 h / -40 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
With
n-butyllithium; ammonium acetate; diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane; acetic acid;
1.1: |Kroehnke Pyridine Synthesis / 1.2: |Kroehnke Pyridine Synthesis;
DOI:10.1002/chem.201203817