Technology Process of C22H10F10N2O
There total 5 articles about C22H10F10N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-pentafluorobenzoyl-5-pentafluorophenyl-1,9-diaza-10,11-dicarbadipyrromethane;
With
sodium tetrahydroborate;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 1.5h;
Inert atmosphere;
With
water;
In
tetrahydrofuran; methanol;
at 20 ℃;
DOI:10.1021/jo2014017
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / 0 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere
3.1: ethylmagnesium bromide / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
3.2: 2.62 h / -78 - 20 °C / Inert atmosphere
3.3: 20 °C / Saturated solution
4.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.5 h / 20 °C / Inert atmosphere
4.2: 20 °C
With
sodium tetrahydroborate; boron trifluoride diethyl etherate; ethylmagnesium bromide; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo2014017
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ethylmagnesium bromide / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
1.2: 2.62 h / -78 - 20 °C / Inert atmosphere
1.3: 20 °C / Saturated solution
2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.5 h / 20 °C / Inert atmosphere
2.2: 20 °C
With
sodium tetrahydroborate; ethylmagnesium bromide;
In
tetrahydrofuran; methanol;
DOI:10.1021/jo2014017