C₃₇H₄₉N₅O₉S₂

Base Information

Chemical Name:C₃₇H₄₉N₅O₉S₂
CAS No.:1308397-59-2
Molecular Formula:C₃₇H₄₉N₅O₉S₂
Molecular Weight:771.956
Hs Code.:

C<sub>37</sub>H<sub>49</sub>N<sub>5</sub>O<sub>9</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₃₇H₄₉N₅O₉S₂

Chemical Property:

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Technology Process of C₃₇H₄₉N₅O₉S₂

There total 10 articles about C₃₇H₄₉N₅O₉S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 154350-29-5
cyclopropanesulphonamide

: C₃₄H₄₂N₄O₇S

: 1308397-59-2
C₃₇H₄₉N₅O₉S₂

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -15 - 20 ℃; for 16h;
DOI:10.1016/j.bmcl.2013.05.046

Reference yield:

: 801282-34-8
N-[(cyclopentyloxy)carbonyl]-3-methyl-L-valyl-(4S)-N-[(1R,2S)-2-ethenyl-1-(methoxycarbonyl)cyclopropyl]-4-hydroxy-L-prolinamide

: 1308397-59-2
C₃₇H₄₉N₅O₉S₂

Guidance literature:: Multi-step reaction with 10 steps

1: dimethylsulfoxide-d6 / 24 h / 55 °C

2: hydrogenchloride; water / methanol / 16 h

3: water; sodium hydroxide / methanol; tetrahydrofuran / 1.5 h

4: triethylamine / tetrahydrofuran / 1.5 h / 0 °C

5: diethyl ether / 1 h / 0 °C

6: hydrogen bromide / tetrahydrofuran; water / 0.5 h / 0 °C

7: tetrahydrofuran / 1 h / 65 °C

8: water; sodium hydroxide / methanol / 16 h / 20 °C

9: isobutyl chloroformate; triethylamine / dichloromethane / 1 h

10: lithium hexamethyldisilazane / tetrahydrofuran / 16 h / -15 - 20 °C

With hydrogenchloride; water; hydrogen bromide; triethylamine; sodium hydroxide; lithium hexamethyldisilazane; isobutyl chloroformate; In tetrahydrofuran; methanol; dimethylsulfoxide-d6; diethyl ether; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.05.046

Reference yield:

: 1308396-66-8
C₂₅H₃₇N₃O₈

: 1308397-59-2
C₃₇H₄₉N₅O₉S₂

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / tetrahydrofuran / 1.5 h / 0 °C

2: diethyl ether / 1 h / 0 °C

3: hydrogen bromide / tetrahydrofuran; water / 0.5 h / 0 °C

4: tetrahydrofuran / 1 h / 65 °C

5: water; sodium hydroxide / methanol / 16 h / 20 °C

6: isobutyl chloroformate; triethylamine / dichloromethane / 1 h

7: lithium hexamethyldisilazane / tetrahydrofuran / 16 h / -15 - 20 °C

With water; hydrogen bromide; triethylamine; sodium hydroxide; lithium hexamethyldisilazane; isobutyl chloroformate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.05.046