C₅₀H₅₂N₂O₂Si

Base Information

Chemical Name:C₅₀H₅₂N₂O₂Si
CAS No.:1379684-23-7
Molecular Formula:C₅₀H₅₂N₂O₂Si
Molecular Weight:741.061
Hs Code.:

C<sub>50</sub>H<sub>52</sub>N<sub>2</sub>O<sub>2</sub>Si

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Chemical Property of C₅₀H₅₂N₂O₂Si

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Technology Process of C₅₀H₅₂N₂O₂Si

There total 7 articles about C₅₀H₅₂N₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1379684-17-9
C₄₇H₅₁NOSi

: 372-09-8
cyanoacetic acid

: 1379684-23-7
C₅₀H₅₂N₂O₂Si

Guidance literature:: With ammonium acetate; In acetic acid; acetonitrile; for 3h; Reflux; Inert atmosphere;
DOI:10.1039/c2jm30978e

Reference yield:

: 953413-02-0
C₃₆H₄₉BrO₂Si₂

: 1379684-23-7
C₅₀H₅₂N₂O₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: bis(tri-tert-butylphosphine)palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / Reflux; Inert atmosphere

2: toluene-4-sulfonic acid / methanol; dichloromethane / 20 °C

3: copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); potassium carbonate; ruphos / tetrahydrofuran; N,N-dimethyl-formamide / 75 °C

4: ammonium acetate / acetic acid; acetonitrile / 3 h / Reflux; Inert atmosphere

With copper(l) iodide; bis(tri-tert-butylphosphine)palladium⁽⁰⁾; bis(η3-allyl-μ-chloropalladium(II)); ammonium acetate; potassium carbonate; caesium carbonate; toluene-4-sulfonic acid; ruphos; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2jm30978e

Reference yield:

: 1250863-85-4
7-bromo-1,2,3,3a,4,8b-hexahydro-4-(4-methylphenyl)-cyclopent-[b]indole

: 1379684-23-7
C₅₀H₅₂N₂O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.75 h / -78 °C / Inert atmosphere

1.2: 25 °C / Inert atmosphere

2.1: bis(tri-tert-butylphosphine)palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / Reflux; Inert atmosphere

3.1: toluene-4-sulfonic acid / methanol; dichloromethane / 20 °C

4.1: copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); potassium carbonate; ruphos / tetrahydrofuran; N,N-dimethyl-formamide / 75 °C

5.1: ammonium acetate / acetic acid; acetonitrile / 3 h / Reflux; Inert atmosphere

With copper(l) iodide; bis(tri-tert-butylphosphine)palladium⁽⁰⁾; bis(η3-allyl-μ-chloropalladium(II)); ammonium acetate; tert.-butyl lithium; potassium carbonate; caesium carbonate; toluene-4-sulfonic acid; ruphos; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile; pentane;
DOI:10.1039/c2jm30978e