1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol

Base Information

Chemical Name:1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol
CAS No.:214541-16-9
Molecular Formula:C₄₅H₆₂N₂O₈Si₂
Molecular Weight:815.167
Hs Code.:

1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<<N-(3-hydroxypropyl)carbamoyl>oxy>methyl>-1,3-propanediol

Synonyms:

Suppliers and Price of 1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol

There total 3 articles about 1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115-77-5
Pentaerythritol

: 214541-16-9
1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / imidazole / dimethylformamide / 0.5 h / Ambient temperature

2: 1.) DMAP / 1.) DMF, room temp., 40 min, 2.) DMF, room temp., 1 h

With 1H-imidazole; dmap; In N,N-dimethyl-formamide;
DOI:10.1021/jo981831e

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 214541-16-9
1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / imidazole / dimethylformamide / 0.5 h / Ambient temperature

2: 1.) DMAP / 1.) DMF, room temp., 40 min, 2.) DMF, room temp., 1 h

With 1H-imidazole; dmap; In N,N-dimethyl-formamide;
DOI:10.1021/jo981831e

Reference yield:

: 530-62-1
1,1'-carbonyldiimidazole

: 156-87-6
propan-1-ol-3-amine

: 214541-15-8
2,2-bis<<(tert-butyldiphenylsilyl)oxy>methyl>-1,3-propanediol

: 214541-16-9
1,3-O-bis(tert-butyldiphenylsilyl)-2,2-bis<<oxy>methyl>-1,3-propanediol

Guidance literature:: With dmap; Yield given; Multistep reaction; 1.) DMF, room temp., 40 min, 2.) DMF, room temp., 1 h;
DOI:10.1021/jo981831e