[RuCl(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-2H))]

Base Information

• Chemical Name: [RuCl(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-2H))]
• CAS No.: 1293364-38-1
• Molecular Formula: C₅₀H₄₁ClN₃O₃P₂Ru
• Molecular Weight: 930.364

Synonyms:

Chemical Property of [RuCl(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-2H))]

Chemical Property:

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Technology Process of [RuCl(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-2H))]

There total 1 articles about [RuCl(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-2H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.86%

trans-[RuCl(NO)(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-H))](perchlorate)*2water → [RuCl(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-2H))] (1293364-38-1)

Guidance literature:

In dichloromethane; byproducts: NO; Irradiation (UV/VIS); irradiation of CH2Cl2 soln. of ruthenium compd. by 60 W tungsten lamp for 15 min; evapn., washing wwith methanol and ether, IR and UV;

DOI:10.1021/om101022p

Reference yield: 40.7%

[RuCl(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-2H))] (1293364-38-1) + sodium perchlorate + water (7732-18-5) + sodium nitrite (7632-00-0) → trans-[RuCl(NO)(triphenylphosphine)2(4-methyl-2-nitro-6-(p-tolyldiazenyl)phenol(-H))](perchlorate)*2water

Guidance literature:

In dichloromethane; water; layering acidified water onto CH2Cl2 soln. of ruthenium compd., adn. of NaNO2, stirring at room temp. for 45 min; separating CH2Cl2 soln., addn. of NaClO4 and methanol, stirring for 1 h,evapn.;

DOI:10.1021/om101022p

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