(3-bromobicyclo[2.2.1]hept-2-en-2-yl)tris(triphenylphosphine)platinum fluoroborate

Base Information

Chemical Name:(3-bromobicyclo[2.2.1]hept-2-en-2-yl)tris(triphenylphosphine)platinum fluoroborate
CAS No.:87518-16-9
Molecular Formula:BF₄*C₆₁H₅₃BrP₃Pt
Molecular Weight:1240.8
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-bromobicyclo[2.2.1]hept-2-en-2-yl)tris(triphenylphosphine)platinum fluoroborate

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Technology Process of (3-bromobicyclo[2.2.1]hept-2-en-2-yl)tris(triphenylphosphine)platinum fluoroborate

There total 4 articles about (3-bromobicyclo[2.2.1]hept-2-en-2-yl)tris(triphenylphosphine)platinum fluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 14104-20-2
silver tetrafluoroborate

: 87518-13-6
trans-bis(triphenylphosphine)bromo(3-bromobicyclo[2.2.1]hept-2-en-2-yl)platinum

: 87518-16-9
(3-bromobicyclo[2.2.1]hept-2-en-2-yl)tris(triphenylphosphine)platinum fluoroborate

Guidance literature:: With PPh₃; In dichloromethane; acetone; Pt complex soln. in CH2Cl2/acetone treated with AgBF4 at 25°C, shaken, centrifuged, decanted, treated with soln. of PPh3 in CH2Cl2; concd. in vac., taken up in CH2Cl2, ether added, mother liquor treated with hexane, ppt. collected, dried in vac., recrystd. (CH2Cl2/hexane); elem. anal.;
DOI:10.1021/om00079a022

Reference yield:

: 87518-05-6
(2,3-dibromobicyclo[2.2.1]hept-2-ene)bis(triphenylphosphine)platinum

: 87518-16-9
(3-bromobicyclo[2.2.1]hept-2-en-2-yl)tris(triphenylphosphine)platinum fluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol

2: PPh₃ / acetone; dichloromethane

With PPh₃; In ethanol; dichloromethane; acetone;
DOI:10.1021/om00079a022

Reference yield:

: Pt(PPh₃)3(C₂H₄)

: 87518-16-9
(3-bromobicyclo[2.2.1]hept-2-en-2-yl)tris(triphenylphosphine)platinum fluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene

2: ethanol

3: PPh₃ / acetone; dichloromethane

With PPh₃; In ethanol; dichloromethane; acetone; toluene;
DOI:10.1021/om00079a022