N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester

Base Information

Chemical Name:N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester
CAS No.:123418-22-4
Molecular Formula:C₃₅H₅₃N₅O₁₆
Molecular Weight:799.83
Hs Code.:

N-(2-O-<benzyl 2-acetamido-6-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2,3-dideoxy-α-D-glucopyranosid-3-yl>-(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester

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Technology Process of N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester

There total 8 articles about N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 67-56-1
methanol

: 110582-59-7
N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine benzyl ester

: 123418-23-5
N-(2-O--(R)-lactoyl)-L-alanyl-D-glutamine methyl ester

: 123418-22-4
N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester

Guidance literature:: With sodium methylate; for 3h; Ambient temperature;
DOI:10.1016/0008-6215(89)84005-4

Reference yield:

: 62853-36-5,71822-09-8,85546-24-3
L-alanyl-(γ-benzyl ester D-isoglutamine)

: 123418-22-4
N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-methylmorpholine, isobutyl chloroformate / 1.) tetrahydrofuran, 15 min, 2.) N,N-dimethylformamide, -15 deg C, 1 h, room temperature, 5 h

2: 48 percent / 0.1M NaOMe / 3 h / Ambient temperature

With 4-methyl-morpholine; sodium methylate; isobutyl chloroformate;
DOI:10.1016/0008-6215(89)84005-4

Reference yield:

: 95900-07-5
benzyl 2-acetamido-6-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-lactone

: 123418-22-4
N-(2-O--(R)-lactoyl)-L-alanyl-D-isoglutamine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / imidazole, tetrahexylammonium benzoate / dioxane / 288 h / Ambient temperature

2: 0.1M NaOMe / 3 h / Ambient temperature

With 1H-imidazole; sodium methylate; tetra-n-hexylammonium benzoate; In 1,4-dioxane;
DOI:10.1016/0008-6215(89)84005-4