Technology Process of C21H25NO3
There total 10 articles about C21H25NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-Benzyloxymethyl-3-oxahept-6-en-1-ol;
With
oxalyl dichloride; dimethyl sulfoxide;
In
dichloromethane;
at -78 ℃;
for 1h;
N-benzyl hydroxylalmine;
In
diethyl ether;
for 1h;
DOI:10.1039/a905802h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 66 percent / copper(I) iodide / tetrahydrofuran / 2 h
2.1: NaH / tetrahydrofuran; various solvent(s) / 1 h / 60 °C
2.2: 61 percent / tetrahydrofuran; various solvent(s) / 4 h / Heating
3.1: 87 percent / LiAlH4 / diethyl ether / 2 h
4.1: dimethyl sulfoxide; oxalyl chloride / CH2Cl2 / 1 h / -78 °C
4.2: diethyl ether / 1 h
With
copper(l) iodide; lithium aluminium tetrahydride; oxalyl dichloride; sodium hydride; dimethyl sulfoxide;
In
tetrahydrofuran; diethyl ether; dichloromethane;
1.1: Coupling / 2.1: Metallation / 2.2: Alkylation / 3.1: Reduction / 4.1: Oxidation / 4.2: Condensation;
DOI:10.1039/a905802h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: NaH / tetrahydrofuran; various solvent(s) / 1 h / 60 °C
1.2: 61 percent / tetrahydrofuran; various solvent(s) / 4 h / Heating
2.1: 87 percent / LiAlH4 / diethyl ether / 2 h
3.1: dimethyl sulfoxide; oxalyl chloride / CH2Cl2 / 1 h / -78 °C
3.2: diethyl ether / 1 h
With
lithium aluminium tetrahydride; oxalyl dichloride; sodium hydride; dimethyl sulfoxide;
In
tetrahydrofuran; diethyl ether; dichloromethane;
1.1: Metallation / 1.2: Alkylation / 2.1: Reduction / 3.1: Oxidation / 3.2: Condensation;
DOI:10.1039/a905802h
