C₁₅H₁₄N₂O₂

Base Information

• Chemical Name: C₁₅H₁₄N₂O₂
• CAS No.: 1245794-39-1
• Molecular Formula: C₁₅H₁₄N₂O₂
• Molecular Weight: 254.288
• Mol file: 1245794-39-1.mol

Synonyms:

Chemical Property of C₁₅H₁₄N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₄N₂O₂

There total 4 articles about C₁₅H₁₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-methyl-2-phenyl-5-(2-furyl)imidazole (1245794-34-6) → C15H14N2O2 (1245794-39-1)

Guidance literature:

With hydrogenchloride; In water; for 2h; Reflux;

DOI:10.1134/S1070427210060194

Reference yield:

1-(2-furyl)-2-bromoethanone (15109-94-1) → C15H14N2O2 (1245794-39-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: methanol / 2 h / Reflux

2.1: ammonium hydroxide; copper diacetate / methanol / 1.5 h / Reflux

2.2: 3 - 8 °C

3.1: hydrogenchloride / water / 2 h / Reflux

With hydrogenchloride; ammonium hydroxide; copper diacetate; In methanol; water;

DOI:10.1134/S1070427210060194

Reference yield:

1-(2-furyl)-1-ethanone (1192-62-7,80145-44-4) → C15H14N2O2 (1245794-39-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: copper(ll) bromide / chloroform; ethyl acetate

2.1: methanol / 2 h / Reflux

3.1: ammonium hydroxide; copper diacetate / methanol / 1.5 h / Reflux

3.2: 3 - 8 °C

4.1: hydrogenchloride / water / 2 h / Reflux

With hydrogenchloride; ammonium hydroxide; copper diacetate; copper(ll) bromide; In methanol; chloroform; water; ethyl acetate;

DOI:10.1134/S1070427210060194

upstream raw materials:

1-(2-furyl)-1-ethanone

1-(2-furyl)-2-bromoethanone

formaldehyd

1-methyl-2-phenyl-5-(2-furyl)imidazole

Refernces