O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate

Base Information

Chemical Name:O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate
CAS No.:126713-97-1
Molecular Formula:C₅₄H₅₅NO₁₆
Molecular Weight:974.028
Hs Code.:

O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate

Synonyms:

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Chemical Property of O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate

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Technology Process of O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate

There total 6 articles about O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110426-17-0
Acetic acid (2R,3S,4S,5R,6R)-5-acetoxy-4-allyloxy-2-allyloxymethyl-6-chloro-tetrahydro-pyran-3-yl ester

: 126713-97-1
O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / silver triflate

2: 91 percent / LiOH/H₂O₂

3: 90 percent / benzylation

4: Wilkinson's catalyst

5: acetylation

With lithium hydroxide; dihydrogen peroxide; silver trifluoromethanesulfonate; Wilkinson's catalyst;
DOI:10.1016/S0040-4039(01)80741-3

Reference yield:

: 125946-67-0
allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

: 126713-97-1
O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / silver triflate

2: 91 percent / LiOH/H₂O₂

3: 90 percent / benzylation

4: Wilkinson's catalyst

5: acetylation

With lithium hydroxide; dihydrogen peroxide; silver trifluoromethanesulfonate; Wilkinson's catalyst;
DOI:10.1016/S0040-4039(01)80741-3

Reference yield:

: 129163-00-4
allyl O-(3,6-di-O-allyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

: 126713-97-1
O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-α-D-glucopyranosyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / benzylation

2: Wilkinson's catalyst

3: acetylation

Wilkinson's catalyst;
DOI:10.1016/S0040-4039(01)80741-3