(N-methylbenzamido)methyl ethanoate

Base Information

• Chemical Name: (N-methylbenzamido)methyl ethanoate
• CAS No.: 135158-61-1
• Molecular Formula: C₁₁H₁₃NO₃
• Molecular Weight: 207.229
• Mol file: 135158-61-1.mol

Synonyms:

Chemical Property of (N-methylbenzamido)methyl ethanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (N-methylbenzamido)methyl ethanoate

There total 1 articles about (N-methylbenzamido)methyl ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-chloromethyl-N-methylbenzamide (51164-42-2) + sodium acetate (127-09-3) → (N-methylbenzamido)methyl ethanoate (135158-61-1)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1023/A:1012146905833

Reference yield:

(N-methylbenzamido)methyl ethanoate (135158-61-1) → N-(hydroxymethyl)-N-methylbenzamide (87489-99-4)

Guidance literature:

With water; In acetonitrile; at 37 ℃; Kinetics;

DOI:10.1023/A:1012146905833

Reference yield:

(N-methylbenzamido)methyl ethanoate (135158-61-1) → N-methylbenzamide (88070-48-8) + N-(hydroxymethyl)-N-methylbenzamide (87489-99-4) + acetic acid (64-19-7,77671-22-8)

Guidance literature:

With phosphate buffer; In acetonitrile; at 20 ℃; for 10h; pH=7.4; Further Variations:; pH-values; Kinetics; Product distribution;

DOI:10.1023/A:1016077200460

upstream raw materials:

N-chloromethyl-N-methylbenzamide

sodium acetate

Downstream raw materials:

N-methylbenzamide

N-(hydroxymethyl)-N-methylbenzamide

acetic acid

Refernces