Phenylmethyl 6-deoxy-3,4-O-(1-methylethylidene)-beta-L-galactopyranoside

Base Information

Chemical Name:Phenylmethyl 6-deoxy-3,4-O-(1-methylethylidene)-beta-L-galactopyranoside
CAS No.:16741-30-3
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:
DSSTox Substance ID:DTXSID001156911

Synonyms:DTXSID001156911;Phenylmethyl 6-deoxy-3,4-O-(1-methylethylidene)-beta-L-galactopyranoside;16741-30-3

Suppliers and Price of Phenylmethyl 6-deoxy-3,4-O-(1-methylethylidene)-beta-L-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Phenylmethyl 6-deoxy-3,4-O-(1-methylethylidene)-beta-L-galactopyranoside

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:294.14672380
Heavy Atom Count:21
Complexity:353

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1C2C(C(C(O1)OCC3=CC=CC=C3)O)OC(O2)(C)C
Isomeric SMILES:C[C@H]1[C@@H]2[C@H]([C@@H]([C@H](O1)OCC3=CC=CC=C3)O)OC(O2)(C)C

Technology Process of Phenylmethyl 6-deoxy-3,4-O-(1-methylethylidene)-beta-L-galactopyranoside

There total 2 articles about Phenylmethyl 6-deoxy-3,4-O-(1-methylethylidene)-beta-L-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16741-29-0
Benzyl-β-L-fucopyranosid

: 77-76-9
2,2-dimethoxy-propane

: 16741-30-3
benzyl 3,4-O-isopropylidene-β-L-fucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 23 ℃; for 6h;
DOI:10.1139/v90-165

Reference yield:

: 77-76-9
2,2-dimethoxy-propane

: 176776-17-3
benzyl L-fucopyranoside

: 16741-30-3
benzyl 3,4-O-isopropylidene-β-L-fucopyranoside

: 71731-75-4
benzyl 3,4-O-isopropylidene-α-L-fucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In acetone; for 24h; Reflux;
DOI:10.1039/d1ra01070k

Reference yield:

: 16741-30-3
benzyl 3,4-O-isopropylidene-β-L-fucopyranoside

: 50611-09-1
benzyl 2-O-acetyl-3,4-di-O-mesyl-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 4 h / 70 °C

2: acetic acid / water / 4 h / Heating

3: pyridine / dichloromethane / 20 h / 0 - 20 °C

With pyridine; acetic acid; In dichloromethane; water;
DOI:10.1039/d1ra01070k