amminedichlorobis(dimethylphenylphosphine)(phenyldiazenido)rhenium(III)

Base Information

Chemical Name:amminedichlorobis(dimethylphenylphosphine)(phenyldiazenido)rhenium(III)
CAS No.:80041-05-0
Molecular Formula:C₂₂H₃₀Cl₂N₃P₂Re
Molecular Weight:655.561
Hs Code.:

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Chemical Property of amminedichlorobis(dimethylphenylphosphine)(phenyldiazenido)rhenium(III)

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Technology Process of amminedichlorobis(dimethylphenylphosphine)(phenyldiazenido)rhenium(III)

There total 1 articles about amminedichlorobis(dimethylphenylphosphine)(phenyldiazenido)rhenium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 20498-24-2,22371-24-0
ReCl₄(P(CH₃)2C₆H₅)2

: 100-63-0
phenylhydrazine

: 30649-37-7
ReCl₂(N₂C₆H₅)(P(CH₃)2(C₆H₅))3

: 80041-05-0,51405-49-3
amminedichlorobis(dimethylphenylphosphine)(phenyldiazenido)rhenium(III)

Guidance literature:: In ethanol; (N2), phenylhydrazine added to a soln. of the Re-complex , heated to 60°C for 0.5 h; reduced in vacuo, hexane added, filtered off, dried in vacuo, elem. anal.;

Reference yield: 40.0%

: 80041-05-0,51405-49-3
amminedichlorobis(dimethylphenylphosphine)(phenyldiazenido)rhenium(III)

: amminedichlorobis(dimethylphenylphosphine)[N,N-methylphenylhydrazido^(2-)-N']rhenium(V) iodide

Guidance literature:: With CH₃I; In tetrahydrofuran; (N2), refluxed for 5 h; volume reduced in vacuo, pentane added, recrystd. from THF-pentane, elem. anal.;