N-(4-CHLOROBENZYL)2-HYDROXYPHENYLSULFAMATE

Base Information

• Chemical Name: N-(4-CHLOROBENZYL)2-HYDROXYPHENYLSULFAMATE
• CAS No.: 392670-36-9
• Molecular Formula: C₁₃H₁₂ClNO₄S
• Molecular Weight: 313.762
• Mol file: 392670-36-9.mol

Synonyms:

Chemical Property of N-(4-CHLOROBENZYL)2-HYDROXYPHENYLSULFAMATE

Chemical Property:

Purity/Quality:

N-(4-CHLOROBENZYL)2-HYDROXYPHENYLSULFAMATE 95.00% ^*data from reagent suppliers

Safty Information:

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Technology Process of N-(4-CHLOROBENZYL)2-HYDROXYPHENYLSULFAMATE

There total 1 articles about N-(4-CHLOROBENZYL)2-HYDROXYPHENYLSULFAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,2-benzdioxathiole-2,2-dioxide (4074-55-9) + 4-chlorobenzylamine (104-86-9) → C13H12ClNO4S (392670-36-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1039/c1ob05442b

Reference yield:

C13H12ClNO4S (392670-36-9) + (S)-2-(aminomethyl)pyrrolidine-1-carboxylic acid tert-butyl ester (119020-01-8) → C12H18ClN3O2S (1316251-36-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane / Reflux

2: trifluoroacetic acid / dichloromethane / 20 °C

With trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane;

DOI:10.1039/c1ob05442b

Reference yield:

C13H12ClNO4S (392670-36-9) + (S)-2-(aminomethyl)pyrrolidine-1-carboxylic acid tert-butyl ester (119020-01-8) → C17H26ClN3O4S

Guidance literature:

In 1,2-dichloro-ethane; Reflux;

DOI:10.1039/c1ob05442b

upstream raw materials:

1,3,2-benzdioxathiole-2,2-dioxide

4-chlorobenzylamine

Downstream raw materials:

C₁₂H₁₈ClN₃O₂S

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