C₂₈H₄₁NO₂SSi

Base Information

Chemical Name:C₂₈H₄₁NO₂SSi
CAS No.:1046470-59-0
Molecular Formula:C₂₈H₄₁NO₂SSi
Molecular Weight:483.791
Hs Code.:

C<sub>28</sub>H<sub>41</sub>NO<sub>2</sub>SSi

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₄₁NO₂SSi

Chemical Property:

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Technology Process of C₂₈H₄₁NO₂SSi

There total 1 articles about C₂₈H₄₁NO₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1046470-56-7
(1S,2S)-2-[(tert-butyldiphenylsiloxy)methyl]-1-[2-((S)-tert-butylsulfinyl)iminoethyl]cyclopropane

: 1826-67-1
vinyl magnesium bromide

: C₂₈H₄₁NO₂SSi

: 1046470-59-0
C₂₈H₄₁NO₂SSi

Guidance literature:: In toluene; at 110 ℃; optical yield given as %de; stereoselective reaction;
DOI:10.1021/ol8013304

Reference yield:

: 1046470-59-0
C₂₈H₄₁NO₂SSi

: C₂₄H₃₃NOSi

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃; for 0.333333h;
DOI:10.1021/jm4002296

Reference yield:

: 1046470-59-0
C₂₈H₄₁NO₂SSi

: 1431768-48-7
C₂₆H₃₅N₃O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydrogenchloride / tetrahydrofuran; water / 0.33 h / 0 °C

2.1: triethylamine / tetrahydrofuran / 27 h / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 7 h

4.1: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / 7.67 h / -78 - 20 °C

5.1: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 20 °C

6.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 18.5 h / 0 - 20 °C

7.1: toluene / 13 h / Reflux

7.2: 1 h / 20 °C

8.1: triethylamine; pivaloyl chloride / dichloromethane / 1.5 h / 0 - 20 °C

9.1: dichloromethane / 1.25 h / 0 - 20 °C

10.1: triethylamine / dichloromethane / 0 °C

With hydrogenchloride; sodium chlorite; 2-methyl-but-2-ene; oxalyl dichloride; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; pivaloyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol; 4.1: |Swern Oxidation / 7.1: |Curtius Rearrangement;
DOI:10.1021/jm4002296