Technology Process of 1-(4-Methoxy-phenyl)-5-methyl-1,3,4,5-tetrahydro-pyrano[4,3-b]indole
There total 8 articles about 1-(4-Methoxy-phenyl)-5-methyl-1,3,4,5-tetrahydro-pyrano[4,3-b]indole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 17.4 g / Heating
2: 9.9 g / melting in vacuo (3 min), distillation
3: 88 percent / LiAlH4 / diethyl ether / 1 h / Ambient temperature
4: acetic acid
With
lithium aluminium tetrahydride;
In
diethyl ether; acetic acid;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 13.7 g / acetic anhydride / 0.5 h / Heating
2: 17.4 g / Heating
3: 9.9 g / melting in vacuo (3 min), distillation
4: 88 percent / LiAlH4 / diethyl ether / 1 h / Ambient temperature
5: acetic acid
With
lithium aluminium tetrahydride; acetic anhydride;
In
diethyl ether; acetic acid;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 16.1 g / KOH / ethanol; H2O / 0.5 h / Heating
2: 13.7 g / acetic anhydride / 0.5 h / Heating
3: 17.4 g / Heating
4: 9.9 g / melting in vacuo (3 min), distillation
5: 88 percent / LiAlH4 / diethyl ether / 1 h / Ambient temperature
6: acetic acid
With
potassium hydroxide; lithium aluminium tetrahydride; acetic anhydride;
In
diethyl ether; ethanol; water; acetic acid;
